[1]王波,张晓艳,黄攀,等.响应面法优化马齿苋黄酮超声波提取工艺[J].江苏农业学报,2018,(01):166-171.[doi:doi:10.3969/j.issn.1000-4440.2018.01.024]
　WANG Bo,ZHANG Xiao-yan,HUANG Pan,et al.Optimization of ultrasonic wave extraction of flavonoid from Portulace oleracea L. by response surface methodology[J].,2018,(01):166-171.[doi:doi:10.3969/j.issn.1000-4440.2018.01.024]
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响应面法优化马齿苋黄酮超声波提取工艺()
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江苏农业学报[ISSN:1006-6977/CN:61-1281/TN]

卷:
期数:
2018年01期
页码:
166-171
栏目:
加工贮藏·质量安全
出版日期:
2018-02-25

文章信息/Info

Title:
Optimization of ultrasonic wave extraction of flavonoid from Portulace oleracea L. by response surface methodology
作者:
王波; 张晓艳; 黄攀; 吕德雅; 严帆; 刘辉
（安徽师范大学环境科学与工程学院，安徽芜湖241002）
Author(s):
WANG Bo; ZHANG Xiao-yan; HUANG Pan; LYU De-ya; YAN Fan; LIU Hui
(College of Environmental Science and Engineering, Anhui Normal University, Wuhu 241002, China）
关键词:
马齿苋; 黄酮; 超声波提取; 响应面优化
Keywords:
Portulace oleracea L.; flavonoid; ultrasonic wave extraction; response surface methodology
分类号:
TS218
DOI:
doi:10.3969/j.issn.1000-4440.2018.01.024
文献标志码:
A
摘要:
以野生马齿苋为试验材料，在单因素试验基础上，采用Box-Behnken试验设计和响应面分析法，探讨乙醇体积分数、液料比、提取时间以及提取温度对马齿苋黄酮提取率的影响。结果表明：优化的马齿苋黄酮超声波法提取工艺条件为乙醇体积分数80%、液料比 30∶1(ml/g)、提取时间55.40 min、提取温度64.19 ℃，此条件下马齿苋黄酮理论提取率为1.42%，实际提取率为1.38%。回归模型的预测值与实测值接近，表明响应面法对马齿苋黄酮提取工艺的优化合理可行。
Abstract:
Using Portulace oleracea L. as material, the effects of ethanol volume fraction, ratio of liquid-to-solid, extraction time and extraction temperature on the extraction yield of flavonoid were determined through response surface methodology based on Box-Behnken experimental design. The results showed that optimum extraction conditions were 80.00%, 30∶1(ml/g), 55.40 min and 64.19 ℃ for ethanol volume fraction, ratio of liquid-to-solid, extraction time and extraction temperature, respectively. Under these conditions, the predicted and actual extraction rates of flavonoid from Portulace oleracea L. were 1.42% and 1.38%, respectively. The predictive value of the regression model agreed with the experimental value, and the optimized conditions for flavonoid extraction from Portulace oleracea L. were reliable.

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备注/Memo

备注/Memo:
收稿日期：2017-05-19 基金项目：国家自然科学基金项目（31400589）；安徽省高校自然科学研究重点项目（KJ2010A150） 作者简介：王波（1974-），女，吉林柳河人，博士，副教授，研究方向为环境生物学、环境与食品安全。(E-mail)wangbohky@163.com
更新日期/Last Update: 2018-03-06